Be897 f73 b0986 f738 a2 d11 ec

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PART 20. (6)(0:C)-SYSTEM
ti
system

^=O

c-e-c:o

N-SHJ: o

o-e-c:o

compound

solv.

4.0

L20

3131

N-me thy Ib enz amide

M

223

4.0

L20

3132

N,N-dimethylbenzamide

M

225

3.8

L20

3133

o-toluamide

M

269

S2g

3134

m-toluamide

M

257

S2g

3135

p-toluamide

M

234.5

S2g

3136

N,N-diethyl-m-toluamide

cH

no

S2g

3137

o- aminobenz amide

M

213
248

S2g

3138

p-amino-N-ethylbenzanilide

A

294-6

4.2

S30

3139

N-ethyl-p-(ethylamino)benzanilide

A

306-7

4.2

S30

3140

p-aminohippuric acid

M

280

S2g

3141

o-hydroxybenzamide

6.0

202.5
236
299

4.6
3.9
3.5

D35

3142

11.0

214.5
241.5
329

4.5
3.9
3.8

D35

3143

222
251
305

4.5
3.7
3.8

W4

3144

240-4

4.3

B45

3145

s-e-c:o

p-carbamoylphenyl disulfoxide

iil

no.

225

a-dihydroacetylcaranine lactam

c-&-e-c:o

ref.

M

O2C-G-CiO

o:c-6— c:o
AtI 4 *

loge

benzamide

N

TT0
TO

max.

A

N-phenylphthalimide

A

294

3.3

F49

3146

N-ethyl-4 , 5-methylenedioxyphthalimide

A

245
302

4.6
3.3

W4

3147

tetrachlorophthalimide

A

234
330

3.9
3.4

R32

3148

tetrachloro-N- [ 2- (dime thylamino) ethyl ]'phthalimide

A

288

R32

3149

2f -methylbiphenyl-2-carbonamide

A

no

F49

3150


compound

system

c-^-.o

f luorene-1-carbonamide

e-c:c-c:o

solv.

A

max.

loge

ref.

no.

262

4.3

F49

3151

cis-cinnamamide

254

4.0

Pl

3152

trans-cinnamamide

273

4.3

Pl

3153

A

288

4.5

S80

3154

*1

288

4.5

S80

3155

*2

288

4.5

S80

3156

240

3.8

Pl

3157

N
N-carbamoylcinnamamide ; cinnamoylurea

w
s
~i '

2-phenyl-l-cyclohexene-l-carbonamide

a- (p-chlorophenyl) -cis-cinnamamide

A

292

4.4

C71

3158

a- (p-chlorophenyl) -trans-cinnamamide

A

223
280

4.4
4.3

C71

3159

e-N:N-c:o

carbamoylazobenzene

A

223
286
434

4.4
4.5
2.6

F44

3160

Br-e-N:N-c:o

l-bromo-4-(carbamoylazo) benzene

A

245
300
440

3.8
3.9
2.1

F44

3161

6-N:N-6-<;:o
A
N-6-N:N-&-c:o

a-(azobenzene-4-carbonamido)phenylacetic
acid

*3

325

M14

3162

a- [ 4 f - (dime thy lamino) azobenzene-4carbonamido]phenylacetic acid

*3

470

M14

3163

a- (4f-hydroxyazobenzene-4-carbonamido)phenylacetic acid

*3

357

M14

3164

N

o-6-N:N-6-c:o

*1

0.01N NaOC2H5M

*2

IN HC1/W

*3

Na salt in W


PART 21. (6)(0:C)- AND OTHER (6)(0:C)-SYSTEMS
6
*
system

compound

solv. ^max.

benzole acid

*£.0

methyl benzoate

phenyl benzoate

c2-6^c:o

3.9

4.0
2.9

M59

3165

cH

231
274.5

4.1
3.0

F49

3166

*1

224
268

3.9
2.7

D33

3167

A

228
273

4.0
2.9

U2

3168

W

230
273

4.1
3.0

U2

3169

A

232

4.2

C33

3170

235
275

4.4
3.4

C73

3171

o-toluic acid

A

205
228
279

4.1
3.7
2.9

M59

3172

m-toluic acid

A

205
232
279

4.1
4.0
3.0

M59

3173

p-toluic acid

A

204
236

4.1
4.1

M59

3174

*2

241.5

4.2

D33

3175

*3

235

4.1

D33

3176

1 , 3-dihydroisobenzof uran-1-one

A

227
273

4.0
3.2

S30

3177

2,6-dimethylbenzoic acid

A

202
270

4.2
2.9

M59

3178

5,6,7, 8-tetrahydro-2-naphthoic acid

cH

243
281

4.2
3.2

F49

3179

2,4,6-trimethylbenzoic acid

A

235
270

3.5
2.6

F5

3180

*4

269

2.5

F5

3181

O

*1

anion

*2

no.

202
228
271

O

c3-e-c: o

ref.

A

benzoyl peroxide

c-6-c:o
6

loge

IN NC1/W

*3

IN NaOH/W

*4

Na salt in A


compound

system

solv.

max.

loge

ref.

no.

methyl 2,4,6-trimethylbenzoate

A

273

2.7

F5

3182

Hg-S-CiO

p-chloromercurybenzoic acid

7.0

232

4.2

B102

3183

N-G-C:O

o-aminobenzoic acid; anthranilic acid

A

218
247
337.5

4.4
3.8
3.7

M56

3184

3.7

216.5
248
327

4.3
3.6
3.3

D35

3185

209
240
310

4.4
3.9
3.4

D35

3186

A

220
320.5

4.3
3.6

M56

3187

3.7

218.5
250
310

4.1
3.4
2.8

D35

3188

11.0

209.5

300

4.4
3.3

D35

3189

A

218
289

3.9
4.3

M56

3190

*1

226.5
270

4.1
3.0

D33

3191

3.7

219.5
284

4.0
4.1

D33

3192

*2

265

4.2

D33

3193

p-(dimethylamino)benzoic acid

A

227

308

3.9
4.4

K77

3194

p-(diethylamino)benzoic acid

A

227
312

3.9
4.5

K77

3195

o-acetamidobenzoic acid

D

252
312

4.1
3.8

Z4

3196

M

251
303

3.9
3.5

G23n

3197

*3

239
315

4.0
3.6

Z4

3198

11.0

m-aminobenzoic acid

p-aminobenzoic acid

3 , 4-dihydro-lH-2-oxa-4-azanaphthalene1,3-dione; isatic anhydride

*1

2N HC1/W

*2

O. IN NaOH/W

*3

dioxane containing 0.01M (CH3)3N


compound

system

M

p-acetamidobenzoic acid

o-6-c:o

solv.

212
267

4.3

3.7
3.7

ref.

no.

S2g

3199

G23q

3200

S2g

3201

H

248
341

ethyl p-aminobenzoate

M

218
289

o-hydroxybenzoic acid; salicylic acid

A

204
236
307

4.4
3.9
3.6

M59

3202

3.0

202.5
237

302.5

4.6
4.0
3.6

D35

3203

9.0

230.5
296

3.9
3.5

D35

3204

11.0

242
306

3.8
3.5

D35

3205

*1

226
294

S2g

3206

A

203
236
301

4.4
3.8
3.4

M59

3207

3.0

206

236.5
296

4.4
3.9
3.4

D35

3208

9.0

287

3.3

D35

3209

216.5
312

4.4
3.4

D35

3210

A

201
251

4.2
4.1

M59

3211

*2

207.5
255

4.1
4.1

D33

3212

8.0

245

4.1

D33

3213

*3

280

4.2

D33

3214

A

206
230
291

4.2
3.8
3.4

M59

3215

m-hydroxybenzoic acid

11.0

p-hydroxybenzoic acid

o-methoxybenzoic acid

ammonium salt in M

loge

methyl o-aminobenzoate; methyl anthranilate

O

*1

max.

*2

O. IN HC1/W

*3

O. IN NaOH/W


compound

system

O2-G-C! O

*1

O. IN HC1/W

*2

solv. ^max.

loge

ref.

no.

m-methoxy ben zoic acid

A

206
230
293

4.4
3.8
3.4

M59

3216

p-methoxybenzoic acid

A

205
249

4.2
4.1

M59

3217

*1

208
256.5

4.2
4.2

D33

3218

*2

247

4.1

D33

3219

o-phenoxybenzoic acid

*3

222
285

4.1
3.5

U5

3220

m-phenoxybenzoic acid

*3

220
290

4.4
3.3

U5

3221

p-phenoxybenzoic acid

*3

255

4.2

U5

3222

o-acetoxybenzoic acid

A

279

3.0

W5

3223

o-benzoxybenzoic acid

A

276

3.3

W5

3224

methyl o-hydroxybenzoate

A

238
306

4.0
3.6

B61

3225

iO

238
308

4.0
3.6

B61

3226

phenyl o-hydroxybenzoate

cH

241
309

S2g

3227

methyl p-hydroxybenzoate

M

255

S2g

3228

methyl o-methoxybenzoate

A

234
294

3.8
3.5

B61

3229

D

231
292

3.8
3.5

B61

3230

methyl p-methoxybenzoate

H

252

S2g

3231

methyl o-acetoxybenzoate

A

279

3.0

W5

3232

methyl o-benzoxybenzoate

A

277

3.3

W5

3233

2,5-dihydroxybenzoic acid

M

216
238

S2g

3234

4-hydroxy-3-methoxybenzoic acid

A

298

LlO

3235

O. IN NaOH/W

*3

cH + D (9:1)


system

*1

cH + D

(9:1)

compound

solv.

max.

loge

ref.

no.

2-hydroxy-3-phenoxybenzoic acid

*1

235
270
316

4.0
3.4
3.7

U5

3236

2-hydroxy-4-phenoxybenzoic acid

*1

260
300

4.2
3.8

U5

3237

2-hydroxy-5-phenoxybenzoic acid

*1

272
327

3.3
3.6

U5

3238

2-hydroxy-6-phenoxybenzoic acid

*1

316

3.8

U5

3239

3-hydroxy-2-phenoxybenzoic acid

*1

277
297

3.4
3.5

U5

3240

3-hydroxy-4-phenoxybenzoic acid

*1

251
295

4.1
3.7

U5

3241

3-hydroxy-5-phenoxybenzoic acid

*1

270
303

3.3
3.6

U5

3242

4-hydroxy-2-phenoxybenzoic acid

*1

252
280

4.3
3.5

U5

3243

4-hydroxy-3-phenoxybenzoic acid

*1

254
285

4.2
3.4

U5

3244

5-hydroxy-2-phenoxybenzoic acid

*1

277

309

3.2
3.5

U5

3245

2,3-dimethoxybenzoic acid

*1

294

3.4

U5

3246

2-methoxy-3-phenoxybenzoic acid

*1

235
270
290

3.9

3.4
3.4

U5

3247

3-methoxy-2-phenoxybenzoic acid

*1

278
295

3.5
3.5

U5

3248

2-methoxy-4-phenoxybenzoic acid

*1

252
291

4.1
3.7

U5

3249

4-methoxy-2-phenoxybenzoic acid

*1

249
280

4.1
3.4

U5

3250

2-methoxy-5-phenoxybenzoic acid

*1

272
327

3.3
3.6

U5

3251

5-methoxy-2-phenoxybenzoic acid

*1

238
277
308

3.9
3.2
3.5

U5

3252


compound

system

O3-G-C! O

6

solv.

max.

loge

ref*

no.

2-methoxy-6-phenoxybenzoic acid

*1

279

3.5

U5

3253

3-methoxy-4-phenoxybenzoic acid

*1

260
295

4.0
3.7

U5

3254

4-methoxy-3-phenoxybenzoic acid

*1

254
285

4.0
3.5

U5

3255

3-methoxy-5-phenoxybenzoic acid

*1

271
301

3.3
3.4

U5

3256

ethyl 3,4-dihydroxybenzoate

D

258
292.5

P5

3257

butyl 4-hydroxy-3-methoxybenzoate

M

217.5
260
291

S2g

3258

4-hydroxy-3 ,5-dimethoxybenzoic acid

A

273

LlO

3259

*2

300

LlO

3260

261
290

S2g

3261

2-methoxy-3 , 4-methylenedioxybenzoic acid M

sec-butyl 4-hydroxy-3, 5-dimethoxybenzoate

M

274.5

S2g

3262

2-hydroxy-m-toluic acid

M

240.5
308

S2g

3263

2-hydroxy-p-toluic acid

M

240
308

3.9
3.6

S2g

3264

oc3-e-c'.o
6

l-acetoxy-7- (diacetoxymethyl) -1 , 3-dihydro-4-methoxy-5-methyl-3-oxoisobenzofuran

A

297

3.7

G33

3265

ON-6-C'.O

4-aminosalicylic acid

A

239
285
304

3.8
4.2
4.2

D37

3266

*3

207
263
295

4.4
4.1
3.9

S2g

3267

4-acetamidosalicylic acid

A

269
304

4.3
4.0

D37

3268

methyl 4-aminosalicylate

A

241
289
307

4.0
4.2
4.3

D37

3269

oc-e-c:o

*1

cH + D (9:1)

*2

0.014% KOH/W

*3

Ca salt in W


system

solv.

max.

loge

m-methylthiobenzoic acid

*1

217
254
302.5

4.2
3.9
3.1

B21

3270

p-methylthiobenzoic acid

*1

276

4.2

B21

3271

so-e-c:o

6-sulf osalicylic acid

M

234
305

S2g

3272

Se-6-C'.O

m-methylselenobenzoic acid

*1

215.5
260
295

4.2
3.8

3.2

B21

3273

p-methylselenobenzoic acid

*1

217
290

3.9
4.1

B21

3274

p-f luorobenzoic acid

M

226.5
263

4.0

S2g

3275

o-chlorobenzoic acid

A

202
278

4.3
2.9

M59

3276

3.0

229
280

3.8
2.9

D35

3277

*2

273

2.4

D35

3278

A

204
230
284

4.3
3.9
3.0

M59

3279

3.0

201.5
231.5
283

4.6

4.0
3.0

D35

3280

*2

228
277

3.8
2.8

D35

3281

A

202
234

4.2
4.2

M59

3282

*3

241

4.2

D33

3283

11.0

235

4.1

D33

3284

2,4-dichlorobenzoic acid

3.0

202
232
282

4.5

3.9
3.7

D35g

3285

2 ,5-dichlorobenzoic acid

M

212.5
225
289

S2g

3286

compound

s-e-c:o
6

F-e-c:o
6
ci-e-C'.o
6

m-chlorobenzoic acid

p-chlorobenzoic acid

ci2-e-c:o
O

*1

5% A/W

*2

O. IN NaOH/W

*3

O. IN HC1/W

ref.

no.


system

compound

solv.

loge

ref.

no.

2 , 6-dichlorobenzoic acid

A

204
274

4.4
2.7

M59

3287

3,4-dichlorobenzoic acid

3.0

205
242
281

4.5
4.1
3.9

D35g

3288

292

3.2

M64

3289

methyl 3,5-dichlorobenzoate

ci3-e-c:o

max.

2,3,4-trichlorobenzoic acid

M

289

2,8

V5n

3290

2,3,5-trichlorobenzoic acid

M

295

3.0

V5n

3291

2,4,5-trichlorobenzoic acid

M

292

3.0

V5n

3292

2,3,4,5-tetrachlorobenzoic acid

M

296

S2g

3293

2,3,5 ,6-tetrachlorobenzoic acid

M

214
294

S2g

3294

ciN-e-c'.o

2-amino-5-chlorobenzoic acid

3.0

218
250
340

4.3
3.7
3.4

D35g

3295

Br-6-C:0

o-bromobenzoic acid

A

205
262

4.2
3.8

M59

3296

m-bromobenzoic acid

A

206
280

4.4
2.9

M59

3297

p-bromobenzoic acid

A

205
240

4.2
4.1

M59

3298

*1

245.5

4.2

D33

3299

*2

239

4.2

D33

3300

ci4-6r-c:o
6

Br2-6-C*.0

2 ,6-dibromobenzoic acid

A

205
262

4.5
3.0

M59

3301

Br O-6-^'.O

5-bromosalicylic acid

W

206.5
308

4.6
3.5

D35g

3302

o-iodobenzoic acid

M

230
279

3.9

S2g

3303

phthalic acid

A

274
281

3.0
3.1

M56

3304

*1

229
276

4.0
3.2

D35

3305

1-^:0

o; ;o

n

*1

O. IN HC1/W

*2

IN NaOH/W


system

solv.. max.

compound

m

£

h°

*1
*5

monosodium salt
copper (I) salt

no.

225
281

4.0
3.1

L23

3306

*2

192.5
227
272

4.6
3.9
2.9

L23

3307

A

227
280

4.2
3.1

M56

3308

*3

209
230
282

4.6
4.1
3.0

D35

3309

*4

277

2.9

D35

3310

A

238

284

4.2
3.2

M56

3311

*2

193
236.5
280

4.6
4.1
3.1

M56

3312

ethyl phthalate

A

223
274

3.9
3.1

H67n

3313

monobutyl phthalate

*5

270

S2g

3314

butyl isophthalate

M

279
288.5

S2g

3315

butyl terephthalate

M

241

S2g

3316

phenyl phthalate

M

^225
^274

S2g

3317

phthalic anhydride

D

251
288

H67n

3318

o-carboxybenzoyl peroxide

M

272

S2g

3319

7-methoxy-6-methyl-l-oxo-2-oxaindan-4carboxylic acid; isogladiolic acid

A

^245
298

G33

3320

bromoterephthalic acid

M

240.5
291.5

S2g

3321

benzene-l,2,4-tricarboxylic acid 1,2anhydride

M

289

S2g

3322

terephthalic acid

o; :o

ref.

*1

isophthalic acid

o:c-6—c:o
6 Ac2 6

loge

*2

disodium salt

*3

O. IN HC1/W

*4

O. IN NaOH/W

3.6
3.3

3.9
3.7


system

:;

°n°

o? 6:0

compound

solv. ^max.

loge

ref.

no.

benzene-l,2,4,5-tetracarboxylic acid

W

297

3.4

B62n

3323

c-6-e-c:o

ethyl f luorene-1-carboxylate

A

245
263

4.4
4.3

F49

3324

6-6-c:o

2-hydroxybiphenyl-3-carboxylic acid

D

230.5
321

S2g

3325

4-hydroxybiphenyl-3-carboxylic acid

M

261.5
321

S2g

3326

biphenyl-2 , 2f -dicarboxylic acid

A

280

3.3 W35

3327

biphenyl-3,3T-dicarboxylic acid

A

no

W35

3328

01 6

methyl biphenyl-4 , 4 f -dicarboxylate

A

280

4.5

W35

3329

4 , 5-methylenedioxybiphenyl-2 , 3T -dicarboxylic acid

A

226
268
295

4.6
3.8
3.8

W35

3330

o:c-e—6 — c:o

2 , 2f , 6 , 6 f -tetrachlorobiphenyl-4 , 4 T -dicarboxylic acid

295

3.6 M64

3331

e-c:c-c:o

cis~cinnamic acid

M

268

4.0 A31

3332

trans-cinnamic acid

A

268

4.3

A31

3333

M

272

4.2

A31

3334

methyl trans-cinnamate

A

216.5
276.5

4.2 M33n
4.3

a-butylcinnamic acid

M

265

S2g

3336

3-methylcinnamic acid

A

265

R19

3337

n

H

o:c-6-6-c:o
O

O

St T

6 ii2 Ci2 6

M: :o

n

^:c^:o
e-c:c-c:o

3335

2-phenyl-l-cyclohexene-l-carboxylic acid

245

3.9

Pl

3338

cH
3- (5 , 6 , 7 , 8-tetrahydro-2-naphthyl) acrylic
acid

228
292

4.2
4.4

F49

3339

methyl 3- (5 , 6 , 7 , 8-tetrahydro-2-naphthy 1)cHacrylate

227
286

4.3
4.4

F49

3340

2-(l,2,3,4-tetrahydro-5,8-dimethyl-lnaphthylidene) prop ionic acid

219
256

4.3
3.0

F49

3341

d c6

c2-6-c: c-c : o
O

C3-^=O


system

compound

:

~ rr
e-c:c-c:o
6 6

~n

loge

ref.

no.

A

222
279

4.3
4.2

B51

3342

ethyl a-benzamidocinnamate

A

222
282

4.3
4.3

B51

3343

*1

301

4.1

M53

3344

*2

230
306

4.0
4.1

M53

3345

A

227
310

4.0

4.2

C4

3346

*3

240
325

4.1
4.1

C4

3347

A

285

4.4

C4

3348

*3

275

4.3

C4

3349

A

327

4.2

C4

3350

*3

335

4.2

C4

3351

*4

253
370

4.0
4.3

C4

3352

A

330

4.2

C4

3353

*3

308

4.2

C4

3354

A

335

4.3

C4

3355

*3

318

4.3

C4

3356

S2g

3357

[enol form of

a-mercaptocinnamic acid

a,af-dithiobis(cinnamic acid)

o2-6~c: c-c : o

max.

ct-benzamidocinnamic acid

ethyl 3-hydroxycinnamate
ethyl benzoylacetate]

: :o

solv.

3 , 4-dimethoxy-a-mercaptocinnamic acid

S O

a-ethylthio-3 , 4-dimethoxycinnamic acid

a,a'-dithiobis (3, 4-dimethoxycinnamic
acid)

ci-&-c:c-9:o

o-chlorocinnamic acid

M

267

ci-e-c:c-c:o

a-acetamido-p-chlorocinnamic acid

A

217
284

4.0
4.3

B51

3358

a-benzamido-o-chlorocinnamic acid

A

220
278

4.3
4.1

B51

3359

a-benzamido-p-chlorocinnamic acid

A

224
284

4.3
4.3

B51

3360

ethyl a-acetamido-p-chlorocinnamate

A

218
288

4.0
4.3

B51

3361

ethyl a-benzamido-o-chlorocinnamate

A

220
279

4.3
4.1

B51

3362

*1

NaOH/W

*2

NaOC2H5/A

*3

0.5N Na2C03/W

*4

5% NaOH/W


system

compound

ethyl a-benzamido-p-chlorocinnamate

solv.

max.

loge

ref.

no.

A

224
288

4.3
4.3

B51

3363

I2o-«:^:o

a-acetamido-4-hydroxy-3 , 5-diiodocinnamic A

acid

245
298

4.4
4.2

B51

3364

c-6-c:c-c:c-c:o
c
6
O3-G-C : c-c : c-c : o

4- (1 ,2 , 3 , 4-tetrahydro-l-naphthylidene) - A
crotonic acid

239.5
324

3.9
4.5

D39

3365

5- (3 , 4 , 5-trimethoxypheny 1) -2 , 4-pentadienoic acid

A

244
319

4.2
4.5

D39

3366

methyl 5- (3 , 4 , 5-trimethoxyphenyl) -2 , 4- A
pentadienoate

249
332

4.2
4.5

D39

3367

a-mercapto-5-phenyl-2 , 4-pentadienoic
acid

A

238
340

3.9
4.3

C4

3368

2 , 2T -dithiobis (5-phenyl-2 , 4-pentadienoic A
acid)

238
325

4.3
4.8

C4

3369

6-c:o-c:c-c:o

(6)(o:c)2(c:c)2-c

(S)(OiC)2(CiC^3-C

6

^:Je°

«:4:?i

4-benzylidene-3-me thy 1-2 -pent enedioic
acid

cH

271

4.2

PIl

3370

4-benzylidene-3-methyl-2-pentenedioic
anhydride

iP

337.5

4.3

PIl

3371

4-cinnamylidene-3-me thy 1-2-pent enedioic
acid

cH

313

4.5

PIl

3372

4-cinnamylidene-3-methyl-2-pentenedioic
anhydride

cH

388

4.6

PIl

3373

a-phenyl-cis-cinnamic acid

A

228
294

4.1
4.4

C71

3374

a-phenyl-trans-cinnamic acid

A

220
274

4.2
4.2

C71

3375

methyl ct-phenyl-cis-cinnamate

A

284

4.3

C71

3376

methyl a-phenyl-trans-cinnamate

A

284

4.2

C71

3377

a- (p-chlorophenyl) -cis-cinnamic acid

A

228
295

4.1
4.4

C71

3378

a- (p-chlorophenyl) -trans-cinnamic acid

A

226
282

4.3
4.1

C71

3379

methyl a- (p-chlorophenyl) -cis-cinnamate

A

288

4.4

C71

3380

methyl a- (p-chlorophenyl) -transcinnamate

A

224
283

4.4
4.3

C71

3381


system

compound

l*-tt°
: :o
°> n
ci-e-c:c-6-c:o

solv.

6-N:N-e-c:o

loge

ref.

no.

2- (carboxymethyl) -3 , 3-diphenylacrylic
acid

A

264

4.0

F49

3382

2- (carboxymethyl) -3 , 3-bis (p-methoxyphenyl) acrylic acid

A

236
278

4.2
4.2

K36

3383

methyl p-(p-chloro-cis-styryl)benzoate

A

236
296

4.2
4.4

C72

3384

methyl p- (p-chloro-trans-styryl)benzoate

A

232
326

4.2
4.6

C72

3385

phenylpropiolic acid

M

247

D41

3386

methyl phenylpropiolate

M

255

D41

3387

azobenzene-4-carboxylic acid

*1

325

M14

3388

4T - (dimethy lamino) azobenzene-2carboxylic acid

9.0

430

4.3

K40

3389

4! - (dimethylamino) azobenzene-3carboxylic acid

9.0

455

4.4

K40

3390

4f - (dimethylamino) azobenzene-4carboxylic acid

9.0

465

4.4

K40

3391

4f -hydroxyazobenzene-2-carboxylic acid

*1

348

M14

3392

4T -hydroxyazobenzene-4~carboxylic acid

9.0

440

K40

3393

*1

355

M14

3394

2-hydroxy-5-methylazobenzene-2 f carboxylic acid

*1

332

M14

3395

2-hydroxy-5-methylazobenzene-4T carboxylic acid

*1

330

M14

3396

azobenzene-4, 4 f -dicarboxylic acid

*2

225
331

^43O

4.1
4.4
3.1

RIl

3397

methyl azobenzene-4 , 4 T -dicarboxylate

A

226
322
427

4.0
4.5
3.0

RIl

3398

azoxybenzene-4 , 4 T -dicarboxylic acid

*2

268
334

4.1
4.3

RIl

3399

O

e-c;c-c:o

max.

O

N-e-N:N-e-c:o

o-6-N:N-e-c:o

oc-e-N:N-6-c:o
O

o:c-6-N:N-6-c:o
6
6

o:c-e-N:N-&-c:o

66
o

*1

Na salt/W

*2

anion

4.3


system

compound
methyl azoxybenzene-4 , 4 f -dicarboxylate

solv. ^max.

loge

no.

RIl

3400

V5

3401

A

^226
266
332

M

230
324

a- (p-carboxyphenyl) -p-methoxycinnamonitrile

M

240
344

4.2
4.5

R31

3402

a- (p-methoxycarbonylphenyl) -p-methoxycinnamon! t rile

M

241
345

4.1
4.4

R31

3403

A

236
322

4.3
4.4

C72

3404

p-chloro-a- (p-ethoxycarbonylphenyl) trans-cinnamonitrile

A

240
307

4.4
4.3

C72

3405

O.C-6-C.O

o-formylbenzoic acid

M

228

S2g

3406

0:0-9-0:0

4-f ormyl-7-methoxy-6-me thy l-l-oxo-2oxaindane

A

269
306

3.9

3.6

G33

3407

2-formyl-4-methoxy~5-methylisophthalic
acid

A

250
300

3.9

G33

3408

*2

271
310

4.0
3.4

G33

3409

o-(p-chlorobenzoyl)benzoic acid

M

256.5

S2g

3410

methyl 2f -f ormyl-4f , 5! -methylenedioxybiphenyl-3-carboxylate

A

242.5
281
324

4.5
3.8
3.8

W4

3411

3-benzoyl-cis-acrylic acid

A

245

4.0

L35

3412

3-benzoyl-trans-acrylic acid

A

238
360

4.1
1.9

J9

3413

*1

244

4.1

J9

3414

A

no

L35

3415

*2

267

4.2

L35

3416

A

258

4.1

L35

3417

*2

262

4.1

L35

3418

(S)2 (O '.9) (N: c) (c :c)-o2 4- (p-inethoxyphenyl) -2- (p-methoxyphenylimino)-3-butenoic acid

(6)2(o:c)(N!C)(c:c)-o
O

(6)2 (0'.C)(NiC) (CiC)-Ci p-chloro-a- (p-ethoxycarbonylphenyl) -ciscinnamonitrile
6

6 Oc2
o:?
0

^"

°cb<:°

o:c-e-e-c:o
6 V

4.3
4.2
4.3

ref.

0.0-*.%*°

3-benzoyl-2-methyl-cis-acrylic acid

"tt***
3-benzoyl-2-methyl- trans-aery lie acid

*1

KOH/A

*2

anion


compound

system

solv.

max.

A

no

*2

246

A
*2

loge

ref.

no.

L35

3419

4.1

L35

3420

245

4.1

L35

3421

250

4.1

L35

3422

3- (2 , 4, 6-trimethylbenzoyl) -trans-acrylic A
acid

296

3.1

J9

3423

A

250
355

4.0
3.6

J9

3424

*1

238
413

4.3
3.5

J9

3425

A

no

L35

3426

*2

275

4.2

L35

3427

A

273

4.2

L35

3428

*2

275

4.2

L35

3429

methyl 3- (p-bromobenzoyl) -2-methyltrans-acrylate

A

277

4.1

L35

3430

3- (p-bromobenzoyl) -cis-crotonic acid

A

no

L35

3431

*2

260

4.1

L35

3432

A

275

4.2

L35

3433

*2

275

4.2

L35

3434

methyl 3-(p-bromobenzoyl)-cis-crotonate

A

262

4.1

L35

3435

methyl 3- (p-bromobenzoyl) -transcrotonate

A

267

4.1

L35

3436

methyl 2-oxo-4-phenyl-3-butenoate

M

227.5
312

3.8
4.2

S64

3437

methyl 2-oxo-4-(p-tolyl)-3-butenoate

M

233.5
324.5

3.8
4.3

S64

3438

methyl 4- (p-methoxyphenyl) -2-oxo-3butenoate

M

241
347.5

3.9
4.3

S64

3439

3-benzoyl-cis-crotonic acid

0!C-CiC*0''0

6

c

3-benzoyl-trans-crotonic acid

o:^0
3- (o-hydroxybenzoyl) -trans-acrylic acid

0:^=0
3- (p-bromobenzoyl) -2-methyl-cis-acrylic
acid

°-n

o-oSrc**

3- (p-bromobenzoyl) -2-methyl-transacrylic acid

Br 6

" >c-o

0!C-ClC^'0
O
C
3- (p-bromobenzoyl) -trans-crotonic acid

e-c:c „.-

:

° f°
c-e-c:c_.
8:
f-°
*+?$*»
0

*1

KOH/A

*2

anion


system

Br-6-CiC

0:

f

compound

methyl 4- (p-bromophenyl) -2-oxo-3butenoate

solv. ^max.

M

loge

ref.

no.

232
318.5

3.9
4.3

S64

3440

240
336.5

3.9
4.4

S63

3441

S2g

3442

Br

o-e-c:6
o:

methyl 3-bromo-4- (p-ethoxyphenyl) -2-oxo- iO
3-butenoate

o:c-6-c:o

N,N-bis (cyanomethyl)phthalamidic acid

g

6

M

N

e-c:o

235
268

4.1
3.9

K44

3443

A

239
267

4.2
3.9

C33

3444

cH

239
270

4.3
3.9

C33

3445

271

328

3.9
3.9

K44

3446

cyclohexyl benzenecarbothiolate

S
phenyl benzenecarbothiolate

227
275

o-6-c:o

cyclohexyl o-hydroxybenzenecarbothiolate

O-6-C'O
C1

o-methoxybenzoyl chloride

cH

272
280

S2g

3447

ci2-e-<: : o

3,4-dichlorobenzoyl chloride

cH

256
263

S2g

3448


PART 22. (G)(OrN)-SYSTEM
compound

system

solv. \nax.

loge

ref.

no.

A

286

3.9

F47

3449

cH

278

4.0

F47

3450

E

284

4.1

F47

3451

o-nitrosotoluene

A

286

3.8

F15

3452

m-nitrosotoluene

A

282

3.8

F15

3453

p-nitrosotoluene

A

314

4.0

F15

3454

C3-S-NiO

2-nitrosomesitylene

A

295
321
790

4.0
4.0
1.3

N3n

3455

N-6-N'.O

N-ethyl-p-nitrosoaniline

A

271-3
415-6

3.7
4.5

S30

3456

N ,N-dimethyl-p-nitrosoaniline

A

273
423

3.8
4.5

K77

3457

B

405

4.4

K68u

3458

*1

357

4.3

B155

3459

N,N-diethyl-p-nitrosoaniline

A

274-6
424-6

3.7
4.5

S30

3460

p-nitroso-N-pheny !aniline

*2

258-60
405-7

3.6
4.3

S30

3461

*3

291-4
390-2

3.7
4.4

S30

3462

p-nitrosophenol [enol form of p-benzoquinone oxime]

*2

302

4.0

M71

3463

p-nitrosoanisole

E

284
323
444

3.7
4.3
-1.8

A21

3464

*3

328

4.1

H71

3465

nitrosobenzene

SHMiO

C-GHMiO

0-6-NiO

Cl-SHMiO

p-chloronitrosobenzene

A

312.5

4.0

T15

3466

ClO-SHMiO

3-chloro-4-nitrosophenol

*2

299

3.8

H71

3467

*3

401

3.3

H71

3468

*1

HC1/W

*2

acid solution

*3

alkaline

solution


system

solv. ^max.

compound

loge

ref.

no.

3-chloro-4-nitrosoanisole

*1

362.5

4.0

H71

3469

Br-S-N.'O

p-bromonitrosobenzene

A

315

4.0

T15

3470

BrO-G-NiO

3-bromo-4-nitrosophenol

*2

304

4.1

H71

3471

*3

401.5

3.8

H71

3472

3-bromo-4-nitrosoanisole

*1

362.5

4.1

H71

3473

p-iodonitrosobenzene

A

332

4.0

T15

3474

3-iodo-4-nitrosophenol

*2

308

4.1

H71

3475

*3

405

4.0

H71

3476

3-iodo-4-nitrosoanisole

*1

362.5

4.0

H71

3477

O:N-G-N:O
62

1 , 3-dihydroxy-2 , 4-dinitrosobenzene

A

235
280
332

3.7
4.1
4.0

E5

3478

*1

*2

i-6-N:o
io-e-N:o

neutral solution

acid solution

*3

alkaline solution


PART 23. (6)(0:N)-SYSTEM
O
system

compound

G-N:O
6

ref.

no.

259.5

4.0

B159n

3479

H

252
280
330

4.0
3.0
2.1

W45

3480

W

202.5
266
325

4.1
3.7
3.1

D35

3481

*1

257

3.8

M52

3482

iO

256.5

3.9

B146n

3483

W

203
273
315

4.2
3.9
3.1

D35

3484

*1

264

4.1

D35

3485

6.0

217
285

3.8
4.0

D33

3486

*1

272

4.1

M54

3487

p-nitrophenylacetonitrile

H

255

4.0

Bl59n

3488

p-nitrophenylacetic acid

A

272

4.0

B152n

3489

a,a,a-trif luoro-m-nitrotoluene

A

247

3.8

S84

3490

a-chloro-p-nitro toluene

H

258

4.1

B159n

3491

a-bromo-p-nitrotoluene

H

264

4.2

B159n

3492

bis (p-nitrophenyl)mercury

A

280

4.7

L6

3493

p-nitrophenylmercuric chloride

A

269

4.7

L6

3494

o-nitroaniline

A

231
276
403-4

4.3
3.7
3.7

S30

3495

*1

275
404

3.7
3.7

D14

3496

*2

223.5

282.5
412

4.2
3.7
3.7

D35

3497

o-nitrotoluene

m-nitrotoluene

p-nitr o toluene

Hg-e-iy:o

loge

A

nitrobenzene

C-GH)I: O
O

solv. ^max.

O

N-S-N: o
6

*1

10% HCl/W

*2

O. IN NaOH/W


system

solv.

ref.

no.

4.2
3.2

S30

3498

233

375

4.3
3.2

D14

3499

*2

226
280
358

4.2
3.7
3.2

D35

3500

A

228-9
371-2

3.8
4.2

S30

3501

*1

230
374

4.1
4.2

D14

3502

*3

226
381

3.8
4.1

D33

3503

N-ethyl-o-nitroaniline

A

232
279-80
425

4.3
3.7
3.8

S30

3504

N-ethyl-p-nitroaniline

A

231-2
386

3.9
4.3

S30

3505

N,N-dimethyl-o-nitroaniline

A

245.5
416

4.3
3.5

M54

3506

W

242
441

4.2
3.3

M54

3507

*4

248
439

4.0
2.8

M54

3508

*5

262

3.9

M54

3509

A

246
400

4.4
3.1

M54

3510

W

247
385

4.2
3.0

M54

3511

*4

247
378

4.2
2.9

M54

3512

*5

251

4.0

M54

3513

compound

m-nitroaniline

p-nitroaniline

N,N-dimethyl-m-nitroaniline

N,N-dimethyl-p-nitroaniline

*1

10% HC1/W

*2

O. IN NaOH/W

*3

IN N'aOH

*4

5eq. HC1/W

max.

loge

A

235
370-7

*1

A

^2OO
386.5

4.2
4.3

M54

3514

W

232.5
422

4.0
4.3

M54

3515

*5

5000 eq. HC1/W


system

compound

solv.

*2

no.

4.0
4.3

M54

3516

*2

^24O

3.9

M54

3517

bis (o-nitrophenyl)amine

A

225
264
417-23

4.2
4.2
4.0

S30

3518

bis (p-nitrophenyl)amine

A

232
402

4.1

4.6

S30

3519

N- (p-nitrophenyl) diphenylamine

A

255
284
394-5

4.0
3.9
4.3

S30

3520

N , N-bis (p-nitrophenyl) aniline

A

231-3
404-5

4.1

4.4

S30

3521

p-nitrophenylbiguanide hydrochloride

W

230
324

M43n

3522

4 , 6-diamino-l , 2-dihydro-2 , 2-dimethyl1- (p-nitrophenyl) -1,3, 5- triazine
hydrochloride

W

240

M43n

3523

o-nitroacetanilide

A

233
270
340

4.2
3.6
3.4

UIc

3524

323-4

4.2

S30

3525

S2g

3526

ethyl p-nitroaniline-N-carbothionate

M

236
333

N-ethyl-N-(o-nitrophenyl)nitrosamine

A

240-2

4.1

S30

3527

N-ethyl-N-(p-nitrophenyl)nitrosamine

A

221-3
312-4

4.0
4.2

S30

3528

bis (p-nitrophenyl)nitrosamine

A

308-10

4.3

S30

3529

3-nitro-o-toluidine

A

235
352.5

4.2
3.1

M54

3530

W

230
345

4.1
3.2

M54

3531

*3

252.5

3.7

M54

3532

A

230
379

3.8
4.2

M54

3533

4-nitro-o-toluidine

5 eq. HC1/W

ref.

^231
422

O

*1

loge

*1

N,NT-diethyl-N,Nf-bis (p-nitrophenyl) urea A

Nc-eny: o

max.

5000 eq. HC1/W

*3

10% HC1/W


system

compound

5-nitro-o-toluidine

6-nitro-o-toluidine

2-nitro-m-toluidine

4-nitro-m-toluidine

5-nitro-m-toluidine

solv.

10% HC1/W

loge

ref.

no.

W

380

4.1

M54

3534

*1

263

3.7

M54

3535

A

231
288.5
373

4.1
3.7
3.2

M54

3536

W

230

292
353

M54

3537

3.6
3.2

*1

273.5

4.0

M54

3538

A

230
283.5
408

4.2
3.7
3.6

M54

3539

W

292.5
416

4.3
3.7

M54

3540

*1

276
416

3.7
3.3

M54

3541

A

236
282.5
404

4.2
3.5
3.5

M54

3542

W

229
285
403.5

4.3
3.6
3.3

M54

3543

*1

258.5

3.7

M54

3544

A

233
373.5

3.9
4.1

M54

3545

W

378

4.1

M54

3546

*1

256

3.8

M54

3547

A

235
287
375

4.2
3.6
3.1

M54

3548

W

228
292
^368

4.2
3.7

3.2

M54

3549

263

3.8

M54

3550

*1

*1

max.


system

compound

3551

W

225

296
410

4.4
3.9
3.8

M54

3552

*1

225
286
416

4.1
3.9
3.5

M54

3553

A

230
280
417.5

4.3
3.8
3.8

M54

3554

W

227
288
428

4.3
3.8
3.7

M54

3555

*1

266

3.9

M54

3556

A

235
373.5

4.2
3.2

M54

3557

W

355

3.1

M54

3558

*1

256

3.7

M54

3559

a,a,a-trifluoro-2-nitro-m-toluidine

A

233.5
395

4.2
3.4

S84

3560

a, a, a-trif luoro-4-nitro-m-toluidine

A

234.5
370

3.9
4.1

S84

3561

*2

245

3.7

S84

3562

A

232.5
4.3
390-400 3.7

S84

3563

*2

232
410

S84

3564

2 ,4-dimethyl-5-nitroaniline

A

230-50
286
370

M54

3565

2 , 4-dimethyl-6-nitroaniline

A

286
425

M54

3566

bis (m-nitrophenyl)phosphinic acid

A

263

J6

3567

O

O
*2

no.

M54

a , a , a-tr if luoro-6-nitro-m-toluidine

10% HC1/W

ref.

4.3
3.9
3.9

3-nitro-p-toluidine

*1

loge

231
286
405

2-nitro-p-toluidine

P-S-N: o

max.

A

6-nitro-m-toluidine

NC2-S-I)I: o

solv.

1OM HC1/A

3.9
3.1

4.2