Agilent InfinityLab LC Series
Preventive Maintenance Checklist
Agilent InfinityLab
Preventive
Maintenance
LC Series
Checklist
Agilent Preventive Maintenance (PM) provides factory recommended service for your systems to
assure reliable operation and the accuracy of your results. Delivered by highly-trained and
certified service engineers using genuine Agilent parts and supplies, Agilent Preventive
Maintenance provides everything you need to reduce unplanned downtime and keep your systems
operating at their peak.
For more information about Agilent Technologies services please visit our web site using the
following URL />
Customer Information
•
•
•
•
Customers should provide all necessary operating supplies upon request of the engineer.
A customer representative should be available to the engineer while performing the
preventive maintenance procedures.
Any parts, not included in the Parts Lists section of this document, are not part of the
recommended Preventive Maintenance service, nor are they included in the price of this
service.
If a system requires the use of additional or special procedures and/or parts for the
instrument service, then these must be ordered separately and charged as a repair, which may
incur additional costs.
Service Engineers Responsibilities
Only complete/printout pages that relate to the system or module being serviced.
Complete empty fields with the relevant information.
Complete the relevant checkboxes in the checklist using a “X” or tick mark “ ” in the checkbox.
Complete Not Applicable check boxes to indicate services that are not delivered as needed.
Complete the PM service in the order of the task listed.
Complete the Service Review section together with the customer. In case of diagnostic tests,
record test results in section service review (test results).
Additional Instruction Notes
•
Please exercise care when using solvents close to the instrument. It could damage the vapor
sensor present in the ELSD.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
System Information
Guidance:
Check box if instrument configuration report is attached instead of completing the table
below.
Instrument System Name/I.D:
Instrument Location:
Record the list of system component product numbers
below.
List the serial numbers of the components present in the
system below.
1.
1.
2.
2.
3.
3.
4.
4.
5.
5.
6.
6.
7.
7.
8.
8.
9.
9.
10.
10.
Preparation
Consult the device user manual for further instructions.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
Module List
Module identification: The module identifier (e.g. G7117A) can be found on the lower right side of
the module front cover.
Module
Instrument Description
G1328B
Manual Injector
G1364F
1260 Infinity II Analytical Fraction Collector
G5628A
Bio-inert Manual Injector
G5654A
Bio-inert Quaternary Pump
G5664B
1260 Infinity II Bio-inert Fraction Collector
G5668A
Bio-inert Multisampler
G7102A
Evaporative Light Scattering Detector
G7104A/C
Flexible Pump
G7110B
Isocratic Pump
G7111A/B
Quaternary Pump VL / Quaternary Pump
G7112B
Binary Pump
G7114A/B
Variable Wavelength Detector
G7115A
Diode Array Detector WR
G7116A/B
Multicolumn Thermostat
G7117A/B/C
Diode Array Detector FS / Diode Array Detector / Diode Array Detector HS
G7120A
High Speed Pump
G7121A/B
Fluorescence Detector / Fluorescence Detector Spectra
G7122A
Degasser
G7129A/B/C
Vialsampler VL/Vialsampler
G7162A/B
Refractive Index Detector
G7165A
Multiple Wavelength Detector
G7167A/B
Multisampler
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7104A/C
G7104A/C Procedure for 1290 Infinity II Easy Maintenance and LongLife Pump Heads
This procedure requires a torque wrench.
Section NOT Applicable
Start "Remove/Install Pump Head" procedure (Agilent Lab Advisor Software).
Remove or lift up solvent inlets in order to avoid solvent spilling.
Remove the pump head assembly.
Follow the steps provided in the 1290 Infinity II Easy Maintenance Pump Head TechNote and
the 1290 Infinity II Long Life Pump Head TechNote.
Replace the pump seals.
Replace the seal wash seals.
Finish "Remove/Install Pump Head" procedure (Agilent Lab Advisor software).
Connect the solvent lines.
Purge the pump with isopropanol.
Replace the high pressure filter frit.
Replace the inline filter frit, if installed.
Replace the seal wash pump cartridge.
Perform pump leak rate test (Agilent Lab Advisor Software).
Perform system pressure test (Agilent Lab Advisor Software).
Save or print-out results.
Reset EMF counters.
G7104A Pump Head Exchange Procedure
Section NOT Applicable
Start "Remove/Install Pump Head" procedure (Agilent Lab Advisor Software).
Remove or lift up solvent inlets in order to avoid solvent spilling.
Remove the classic pump head assembly.
Install the Infinity II Easy Maintenance pump head assembly.
Finish "Remove/Install Pump Head" procedure (Agilent Lab Advisor software).
Replace the high pressure filter frit.
Replace the inline filter frit, if installed.
Replace the seal wash pump cartridge.
Connect the solvent lines.
Purge the pump with isopropanol.
Perform pump leak rate test (Agilent Lab Advisor Software).
Perform system pressure test (Agilent Lab Advisor Software).
Save or print-out results.
Reset EMF counters.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7104A Alternative Procedure (Classic Pump Heads)
This procedure requires the 1290 Infinity Pump head service kit.
Section NOT Applicable
Start "Remove/Install Pump Head" procedure (Agilent Lab Advisor Software).
Remove or lift up solvent inlets in order to avoid solvent spilling.
Remove the pump head assembly.
Follow the steps provided in the Agilent 1290 Infinity Pump Head Maintenance Technote
Replace the pump seals.
Replace the seal wash seals and gasket.
Finish "Remove/Install Pump Head" procedure (Agilent Lab Advisor software).
Connect the solvent lines.
Purge the pump with isopropanol.
Replace the high pressure filter frit.
Replace the inline filter frit, if installed.
Replace the seal wash pump cartridge.
Perform pump leak rate test (Agilent Lab Advisor Software).
Perform system pressure test (Agilent Lab Advisor Software).
Save or print-out results.
Reset EMF counters.
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Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7110B, G7111A/B, G5654A
Section NOT Applicable
Power off the pump.
Remove pump head.
Disassemble the pump head.
Remove and clean pistons.
Clean support rings.
Replace piston seals.
Replace wash seals and gaskets, if the seal wash option is installed.
Reassemble the pump head and install it.
Reconnect the AIV to the connector (if installed).
Replace the seal wash peristaltic pump if active seal wash is installed.
Power on the module.
For standard (PTFE) or PE seals perform the seal wear-in procedure.
While running, begin maintenance on the sampler and column compartment if applicable.
Purge valve: replace the PTFE frit, replace the seal cap assembly.
If seal wash option is installed: Review the correct installation of seal wash function in
non-recycle mode. Manually activate the seal wash and check if there is a flow.
Perform the System Pressure Test (Agilent Lab Advisor software).
Perform the Leak Rate Test (Agilent Lab Advisor software).
Save or print-out results.
Reset EMF counters.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7112B
Section NOT Applicable
Power off the pump.
Remove pump heads.
Disassemble the pump head.
Remove and clean pistons.
Clean support rings.
Replace piston seals.
Replace wash seals and gaskets, if the seal wash option is installed.
Reassemble the pump heads and install them. Reconnect the Active Inlet Valves to the
connectors.
Replace the seal wash peristaltic pump if active seal wash is installed.
Power on the module.
For standard (PTFE) or PE seals perform the seal wear-in procedure.
While running, begin maintenance on the sampler and column compartment if applicable.
Purge valve: replace the PTFE frit, replace the seal cap assembly.
If seal wash option is installed: Review the correct installation of seal wash function in
non-recycle mode. Manually activate the seal wash and check if there is a flow.
Perform the system pressure test (Agilent Lab Advisor Software).
Perform a Pump Leak Rate Test (Agilent Lab Advisor software)
Perform a pump elasticity calibration (Agilent Lab Advisor Software).
Save or print-out results.
Reset EMF counters.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7120A
G7120A Procedure for 1290 Infinity II Easy Maintenance and LongLife Pump Heads
This procedure requires a torque wrench.
Section NOT Applicable
Start "Remove/Install Pump Head" procedure (Agilent Lab Advisor Software).
Remove or lift up solvent inlets in order to avoid solvent spilling.
Remove the pump head assembly.
Follow the steps provided in the 1290 Infinity II Easy Maintenance Pump Head TechNote and
the 1290 Infinity II Long Life Pump Head TechNote.
Replace the pump seals.
Replace the seal wash seals.
Replace the filter frit (PTFE frits (pack of 5) (01018-22707)) and seal cap (Seal cap
(5067-4728)) of the high pressure filter assembly.
Finish "Remove/Install Pump Head" procedure (Agilent Lab Advisor software).
Connect the solvent lines.
Purge the pump with isopropanol.
Replace the seal wash pump cartridge.
Perform pump leak rate test (Agilent Lab Advisor Software).
Perform the system pressure test (Agilent Lab Advisor Software).
Save or print-out results.
Reset EMF counters.
G7120A Pump Head Exchange Procedure
Section NOT Applicable
Start "Remove/Install Pump Head" procedure (Agilent Lab Advisor Software).
Remove or lift up solvent inlets in order to avoid solvent spilling.
Remove the classic pump head assembly.
Install the Infinity II Easy Maintenance Pump Head assembly.
Finish "Remove/Install Pump Head" procedure (Agilent Lab Advisor software).
Connect the solvent lines.
Purge the pump with isopropanol.
Replace the seal wash pump cartridge.
Perform pump leak rate test (Agilent Lab Advisor Software).
Perform the system pressure test (Agilent Lab Advisor Software).
Save or print-out results.
Reset EMF counters.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7120A Alternative Procedure (Classic Pump Heads)
This procedure requires the 1290 Infinity Pump head service kit
Section NOT Applicable
Start "Remove/Install Pump Head" procedure (Agilent Lab Advisor Software).
Remove or lift up solvent inlets in order to avoid solvent spilling.
Remove the pump head assembly.
Follow the steps provided in the Agilent 1290 Infinity Pump Head Maintenance Technote
Replace the pump seals.
Replace the seal wash seals and gasket.
Replace the filter frit (PTFE frits (pack of 5) (01018-22707)) and seal cap (Seal cap
(5067-4728)) of the high pressure filter assembly.
Finish "Remove/Install Pump Head" procedure (Agilent Lab Advisor software).
Connect the solvent lines.
Purge the pump with isopropanol.
Replace the seal wash pump cartridge.
Perform pump leak rate test (Agilent Lab Advisor Software).
Perform the system pressure test (Agilent Lab Advisor Software).
Save or print-out results.
Reset EMF counters.
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Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7129A/B/C
Section NOT Applicable
Verify the proper function of the drawers.
Replace the rotor seal.
Replace the needle assembly and the high pressure needle seat assembly.
Replace the peristaltic pump cartridge.
Check the finger of the vial gripper.
Verify the proper installation of the sample loop. Especially check if sample loop is moving
smoothly with the safety cover installed.
Check the proper function of the needle wash. Verify correct positioning of the drain tube.
Clean the instrument, especially the ventilation.
Clean the ICC heater (if applicable).
Clean the Sample Cooler, especially the ventilation and verify that the drain tube is positioned
correctly (if applicable).
Clean the Sample Thermostat, especially the ventilation and verify that the drain tube is
positioned correctly (if applicable).
After maintaining the multicolumn thermostat or the ICC heater, purge both modules with
isopropanol for 5 min.
Cap the outlet of the vialsampler with a blank nut ( Blank Nut SL (5067-6127)).
Perform a System Pressure Test.
Perform a System Pressure Test with ICC heater (if applicable).
Perform a Sample Cooler Test (if applicable).
Perform a ICC Heater Test (if applicable).
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Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G1328B/G5628A
Section NOT Applicable
Replace rotor seal.
Replace the stator face assy (G1328C: valve 5067-4191, G5628A: valve 5067-4158).
Purge injector and column compartment with isopropanol for 5 min.
Cap the valve outlet with a blank nut.
Perform a (System) Pressure Test. Take care for the maximum pressure of the valve and
installed loop. (PEEK loop max. pressure is 200 bar).
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Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7167A/B, G5668A
Section NOT Applicable
Verify the proper function of the drawer(s).
Check the needle position of the Multisampler (see LadAdvisor: Instrument control > Special
Commands > Check Needle position). If the needle tip position is off the center perform an
auto referencing under operating conditions.
Replace the rotor seal(s).
Replace the needle assembly(ies) and the high pressure needle seat assembly(ies).
Verify the proper installation of the sample loops especially check if sample loops are kinked
or bended.
Replace the peristaltic pump cartridge (if applicable).
Check the proper function of the needle wash and seat backflushing (if applicable). Verify
correct positioning of the drain tube.
Clean the instrument, especially the ventilation.
Clean the Sample Cooler, especially the ventilation and verify that the drain tube is positioned
correctly (if applicable).
Clean the Sample Thermostat, especially the ventilation and verify that the drain tube is
positioned correctly (if applicable).
After maintaining the multicolumn thermostat, purge both modules with isopropanol for
5 min.
Cap the outlet of the multisampler with a blank nut ( Blank Nut SL (5067-6127)). If this blank
nut is not immediatly availabe perform the test with the TCC included.
Perform a System Pressure Test (for a dual needle system you have to check the left and the
right flow path).
Perform a Sample Cooler Test (if applicable).
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7116A/B
Section NOT Applicable
Before disconnecting the columns, please record the columns and their position as a reference
for re-installation.
If a valve is installed, replace the rotor seal (see parts section for details).
Purge LC system with HPLC grade water for 10 min.
Perform a System Pressure Test. Use a ZDV to install a blank nut onto the heat exchanger's
outlet capillary. If a valve is installed use the blanking nut to block one of the outlet ports. In
case of a column selector valve use a ZDV-union to mount the blanking nut on the outlet port
capillary with the valve switched to the bypass channel.
Reset EMF counter (Valve switches).
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7114A/B
The maintenance procedure requires NO consumables.
Section NOT Applicable
Inspect flow cell for leaks.
Perform holmium oxide test.
Perform Intensity Test.
Perform Wavelength Verification Test.
Perform Dark Current Test.
Perform Filter Test.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7115A, G7165A
The maintenance procedure requires NO consumables.
Section NOT Applicable
Inspect flow cell for leaks.
Perform Filter Test and attach results to checklist.
Perform dark current test.
Perform holmium oxide test.
Perform Intensity Test.
Perform Slit Test.
Perform Wavelength Verification Test.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7121A/B
The maintenance procedure requires NO consumables.
Section NOT Applicable
Inspect the tubing from cell outlet to waste (must be a PTFE tubing without restriction).
Inspect flow cell for leaks.
Perform the lamp Intensity Test and compare profile (no given limits).
Perform the wavelength verification test using the raman band.
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7162A/B
Section NOT Applicable
Purge the reference and sample cells with water for 5 min.
Check diode balance with pure water in both, the reference and the sample cell, instrument
stable as specified. Adjust optical balance if value >±0.2 .
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7117A/B/C
The maintenance procedure requires NO consumables (2x Position Cell Drawer Assembly
G4212-40007 (Replace only if worn))
Section NOT Applicable
Inspect flow cell for leaks.
Check the condition of the positioner cell drawer assembly.
Perform Wavelength Verification Test.
Perform Intensity Test.
Perform Dark Current Test.
Perform Slit Test (not available in G7117A/C).
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7102A
Section NOT Applicable
Check communication of Control Software with the instrument
Mass Flow Controller - Check control of gas flow
Lamp Assembly - Check change in baseline from standby to run.
Photo Detector Module - Check change in baseline from standby to run
Check autozero function
Evaporator Heater Assembly - Check evaporator temperature increases/decreases
Nebuliser Heater Assembly - Check nebuliser temperature increases/decreases
Peltier Assembly (on G7102A cooled only) - Check for cooling to sub-ambient temperatures
Clean optics block assembly if baseline noise greater than 3 LSD units
If cleaning the Optics did not achieve the results then proceed with the cleaning of the prism
assembly.
Check for dust around cooling fan, and clean if necessary
Replace the following parts:
Evaporator Cartridge
Gas Inlet Plug Assembly
Clean the Nebuliser Assembly if cleaning prism and optics assembly, and replacing above
parts does not resolve baseline noise issues
Return the instrument to initial conditions.
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Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G1364F, G5664B
Section NOT Applicable
Replace the Inlet / Waste tubing.
Replace the Valve to Needle tubing.
Perform a Delay Calibration.
Perform a checkout method with the following settings:
Sample:
Delay Calibrant 5190-8223
Eluent A:
0.1 % TFA in LC grade water
Eluent B:
0.1 % TFA in ACN
Flow:
25 mL/min (5 mL/min on 9.4 mm column)
Gradient:
0.0 min
98 % A
2%B
0.3 min
98 % A
2%B
3.5 min
2%A
98 % B
4.2 min
2%A
98 % B
4.3 min
98 % A
2%B
5.5 min
98 % A
2%B
Runtime:
5.5 min
Injection volume:
50 µL (10 µL on 9.4 mm column)
Peak Detector:
UV or DAD signal A, UV 310 nm (+/- 4 nm, 5 Hz, no reference)
Peak Det. Mode:
Threshold (5 mAU) and Slope (50 mAU)
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
Guidance
If the PM service is performed prior to a qualification service, then use the qualification
procedure as a guide for final instrument set up and checkout.
Service Review
Attach available reports or printouts to this documentation.
Record the PM service activity in the customer’s instrument records/logbook
Update/reset instrument maintenance counters as appropriate
Affix the PM sticker to the system or instrument logbook based on the customer’s request.
Complete the Service Engineer Comments section below if there are additional comments.
Review the service and any test results with the customer.
If the instrument firmware was updated, record the details of the change in the Service
Engineer Comments box below or if necessary, in the customer’s IQ records.
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Agilent InfinityLab LC Series
Preventive Maintenance Checklist
Pump Test Results Table
Section NOT applicable
Test Description
Expected Test Result
System Pressure Test
Pass
Leak Rate Test (1260 Infinity II pumps)
Pass
Pump Leak Rate Test
Pass
Pump Self Test (if necessary)
Pass
Pump elasticity calibration (G7112B)
Pass
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Actual Test Result
Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7104A/C, G7120A Parts List Table
Section NOT applicable
Part Description
Product/Model #
where used
Easy Maintenance Pump Head Channel
A
G4220A
Easy Maintenance Pump Head Channel
B
G4220A
Easy Maintenance Pump Head Quat
G4204A
Part Number
Quantity
Consumed
G4220-60300
G7120A
G4220-60310
G7120A
G4204-60300
G7104A
Long Life Pump Head Channel A
G4220A
G4220-60350
G7120A
Long Life Pump Head Channel B
G4220A
G4220-60360
G7120A
Long Life Pump Head Quat
G4204A
G4204-60350
G7104A/C
Wash Seal PE
1100/1200 Series Pumps
0905-1718
1200 Infinity Series
Pumps
InfinityLab LC Series
Pumps
all 1120 and 1220
systems
PE seals (pack of 2)
1100/1200 Series Pumps
0905-1420
1200 Infinity Series
Pumps
InfinityLab LC Series
Pumps
all 1120 and 1220
systems
Gasket, seal wash (pack of 6)
G7104A/C
5062-2484
G7120A
PTFE frits (pack of 5)
G7120A
01018-22707
Frit for pump outlet filter 2/pk
G7104A/C
5067-5716
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Agilent InfinityLab LC Series
Preventive Maintenance Checklist
Part Description
Product/Model #
where used
Part Number
Frit 0.3 µm for inline filter, 5/pk
G7104A/C
5023-0271
Peristaltic pump with Pharmed tubing
1100/1200 Series Pumps
5065-4445
Quantity
Consumed
1200 Infinity Series
Pumps
InfinityLab LC Series
Pumps
1100/1200 Series
Autosamplers
1200 Infinity HiP
Samplers
InfinityLab LC Series
Samplers
PM Kit for LL/EM Heads (Quat. Pumps)
G7104A/C
G7104-68741
G4204A
PM Kit for LL/EM Heads (Binary
Pumps)
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Revision: 3.4
G7120A
G7120-68741
G4220A
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Agilent Technologies
Agilent InfinityLab LC Series
Preventive Maintenance Checklist
G7110B, G7111A/B, G7112B, G5654A Parts List Table
Section NOT applicable
Part Description
Product/Model #
where used
Part Number
1260 Iso/Quat/1220 Pump PM kit
includes seal cap assemblies, standard
piston seals, film washers and PTFE
frits (use this kit for reversed phase
applications)
G7110B
1260 Binary Pump PM kit includes seal
cap assemblies, standard piston seals,
film washers and PTFE frits (use this kit
for reversed phase applications)
G7112B
G1312-68741
PM Kit for Bio-inert Quaternary Pump
includes bio-inert piston seals, seal cap
assemblies, film washers, bio-inert
wash seals, PTFE frits and the
peristaltic pump.
G5654A
G5611-68741
Seal Wash PM kit for 1260 Pumps
includes film washers and standard
wash seals.
G7110B
G1310-68742
Quantity
Consumed
G1310-68741
G7111A/B
G7111A/B
G7112B
Peristaltic pump with Pharmed tubing
1100/1200 Series Pumps
5065-4445
1200 Infinity Series Pumps
InfinityLab LC Series Pumps
1100/1200 Series
Autosamplers
1200 Infinity HiP Samplers
InfinityLab LC Series
Samplers
PE seals (pack of 2)
InfinityLab LC Series Pumps
0905-1420
Wash Seal PE
1100/1200 Series Pumps
0905-1718
1200 Infinity Series Pumps
InfinityLab LC Series Pumps
all 1120 and 1220 systems
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