Thiết kế phân xưởng sản xuất biodiesel từ dầu hạt cao su




 !"#$%&'() *!+ &, /"
 01*)23#4"/)5 '6"/) 22' &55
#727/&!!(8&9*9 :/!"/)  ;( 
<#727/=&>#727/2/!, /'"/)5 :. *?
#$#727/(@&>2-.  A#$%! A#$ B*C D
&,*C @:*) E"/)/.#$ & .@6. /!
/'#$(F&>6+G/'. 2H  B""  /6
#727/25 I&>2-. *?@: .@2*?#727/& A
#$%
J)*41&!/! ; (;@E-K2-. #727/ A#$ B*C
&>/!#$' 2E/!/'#$(&>23#4 B@L6/'
5 +/>/?K) J)&M*!&5. "G2-.
#727/ A"/)!/'(; N&(:/)I2-.
#727/ A#$ B*C 5@@@6 &5@@@&>23#4
. /! B)@O &P72 7"6&I ;!@O!
/'5(Q C (6#&5@/B)2-. #727/
@R>@*?"/)6&S "(Q C *! :( ;1N
T)!&> B) "2K TI6&&$&1 PN/U ;
*!, 2(; N B)&M&>
) B)&/!, ,  &I2*") 5(;
O&MV/!N7*?*)/B6 :  ; 9  B ;
EV/!?&$ "&I2*"/!N7*?*)1, (Q2 
/


*" B)
W'XY


W'XYZ


 Z
. 
[[? )*<#727/ \
 [[[<#727/*! $N \
[[Z:. 1#727/]
[ZJ"/)2-. #727/^
 [Z[_N "/)2-. #727/ ^
[ZZ? )#$' 2 `
 [Zab3/U2,"/) [c
[ad@@@ P>@#727/  [Z
[a[W@@2.5@@@) @E [Z
[aZW@@@/M [Z
[aaW@@(-G  [Z
 [aeW@@V 5 [Z
[a\W@@ &P72 7 [Z
[eP>@#727/ 7@@@ &P72 7[a
 [e[<. 5 [a
[eZE@O &P72 7 [e
 [ead;@O [e
[eed@@@ B)@O &P72 7 []
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/>@ ) !! F T 
0. &,'V F 7*C6"/)$@&' "$.
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E2 ;?!! F6@/B*F/>*! 0!
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2-. "/)2'!&GU. "/)2<#727//!,
#'"/)2&>N E#-?#727/5&, "
!$
<#727//!/(/72 71- o6, @4.   "/)#727/&I
/!&(I(: &,'p
Z
6dp6dp
Z
q(:!(:r6#
; 6s& t*!/!"/)5(F  '&>
)@  I"/)2#727/2uG@K,F/>6
2B@4 ,*!"/)5 '6& 0&7/'*)/!*!/>C
0#Ev[w
EFG4F6FHBI29:2;<;=
<#727/ 0&>&;k@O &P72 772 751
/-7 6-  B#*?>C. &O' Ad[jde@E 3
/-7 6/-7/&96S(- od- o(
5+ :. *C /U*!5(&56 !@$- o/!
; N 6N; &9 :. 1#$6D
_I5 /-7  !#727/6. G- o( 

&P6"6 !@$- oN; &9/ :. 1#727/T*C6
#727/&>-7/!/(/72 76 #4. /!7 /72 7 ' ! A#$
D&, B*C d- o #$6D52 &*?@E
35 #727/(6+. G1+- !/!' 8"S
2-7 EV/!/U#:&I#$ B*C 6D&,*C /!"
W'XY\

/)2-. #727/
#727/!/>/Y.  .@6(O>@.  *!
!/>-(<#727/(6. #m9-5#5!/>/?
>@. (q- o(rvZw
5 I .x :. 1#727/N>&I(23
#42*?#727/(
&J"9<K@L4<M4EFG4FHBI29:2;<;=732:2;<;=N9KOP
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<#727//!/(/72 7' 8#*C"/)!5 92-7 
#727/(6&@O"$1+&,&=%"/). />
*?(F Bg !($@4 F 92-7 
#727/!/>/Y.  .@6(c6cc[{6/!&(I
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EF= ; 9*!Em 0
 <#727/O([[{-"N T1"/)-!
!62B ',6&5s &,*!2B@  #6dp6dp
Z

&(I
<#727/5(F " .   #&5#727/=/!, @4
.   #727/(6G@'2B!=&,
d5(F@E12. qh`{ *=Z[!r6(g@4
&>2BEm(  0
 <#727/5) &,?@q "[[c

dr62*?#727/

(q(]c
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dr6#*C !  O*!*CI<#727//!
F/>  '&>0 6&,/C@*?#$%6(/!2;
F/> B"v[w
W'XY]

ITFR2S@
 <#727/ &> A#$ B*C 5 !(2*?#727/(
J N T2-. 5 I '2@L@4/-75 9 
'/?R/'@$!1#727/v[w
!@$5!/>-") 1#727/ .@2*?
#727/(6#*C "/) "RNM&0vZw
<#727/5 I 's T"/)# :#m9-5}/!'
*=&)2#2B(  :1#727/*?. /)/!
*=&)
J) &,&&s1#727/@4 ,*!"/)2-. 5
/!2*?#$#727/  0!K. /?&;*)
23#4#727/K+*R5 0 ; /'va6ew
J"/)#$ B*C 5 :.  0*4V2B(P&9*
+/>*!. />1, 2"/)(D6D=t/!
, ';1#727/#&5$N'  "/)
i>Jp
-
 (: (q[c{r*!;N T2-. (&
T*l5 IEm#-!@=6(67 /#t*C@5 "
L4 I&I&. />#727/v[w
d:*T(F@E12*!#m9-5#&5$GU&s
)  *.&N O#27/
6UV=256<JW6G4I29:2;<;=

/K2A6K4FKF6X6UV=256<JW6G4I29:2;<;=OP
d"/)&I2-. #727/5 I/!/'#$ B*C #$6
#$&C!6#$' 6#$#A6#$' 2t6/'D&,*C 
D6D=R ,*!&()1 AN!5 I2-. #727/
A"/)(d8'K~Q60 1;2-.
#727/ A#$&C!6KdE•2-. #727/ A#$' 
€? 5*!4/'#$ B*C *?2/> &/?#R
)@ #$*!-. (L#$#A6#$/'6#$*At2&51;/!
#$#A?&E6#$#A1;#R&I2-. , 2 B@L*!-. (L
2X(P&9*2/>V. />)23
#$#A&I '#727/2u/!?&?5)N
W'XY^

J!#$ B*C 6!F?  &>, />. /? 6
2 *!25 ?[\6^÷Za6h{/!D6*)23#4D&I2
-. #727/2u &>/>C*!5@@$ Im 0
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' 2Oec÷\c{/!#$5!EKE' ' 25T
7/@- *?(:D6#!Z6\ja' 56sZ÷ez' 6 "' 5

.E
\' E2
!F6( `s h/! 0&I2 ,. *?
F2. ([ .' z7 (" " ;?6(o@[ .' 6 T
2u &>[cc(#$' 2$' 25O&, /f #?#'
-6>@. !#? #417f&s)s  0-
;2uI5 !>@. -&5#$2( I23#4&>
 B@L$' 2V5(F;;7 /72 7/'
#$ B*C (&I23#4 )@%?  "&. &> **!
/.E' J+E' !&>2.(&I L&56' &>&
*!*!#$&>//.$N/2u&>#R/!"/)&I
2-. #727/
W'XY`

\•#41' 2
d2K 1s 1o@' 2/.#$ 0*?)2.
([^{/!. *!‚2KS/!(*! .'  , !6s
(#"/)(P&9q2 ,S (Z
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(Z\cc&z(r
 I23#4)N' 2&5 @&P?); 6 
k F)2. /"ac{*!N&5 5 I#R#$!&I2-. 7 /72 7
 !([cccc&z/: . /> &*?. />
7 /72 71#$&C!!K~Q&2-. 23#4*!-. (L*? "
'/! 
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W'XYh
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/)#727/:/!&,? ‰K1&,? /!) .@"
/)1&,/!*)(T 06". />1N T@*!
(od. />1N T@*!(o"S "1&,
#727/2u(o&(23#4#$ B*C &56@@/!&,?
&>N E ? "v\w
W'XY[[

,i]K]<GUaBU]]K]254]j
WE1@E 3#$ B*C k) (5s 1-2u '‚
>@/(6/(#76- -/6>@.  *!(:)@@@
!: 23#4*T( :>@6)2.  #727/ .@6$5) &, "
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E/!@@@&6#m#! B)KNW ,&> ;
!k@@@6(&=% ; 9@O '@6‚>@C&>
*+*!P&9  0#!J>&I1@@@!/!( y/)
#$ B*C /?\c{ T( :>@6*T/G!&,? 1‚>@/?
&,? #727/_@/M#727/k#$ B*C 6‚>@[c{#$ B
*C 5&,?  &P(&(I2*?#727/*! I) :F(Q C  
&*?&,#727/vZw

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T/!g g'#1#$ B*C #? #41) *!.
-G  :>@@L1N T(#$ B  0
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' ([\cŠ&>@E& V 
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/!N T @#m#!*!  K@2. (:NI=2@L&
1•[q[Zr&*! @. E(qdr&I #727/d. @
2. (:NI&*?+. 3s&=%$5) &,6"5 I-
+@O( ?(. 3!&56@2. .
&>/![c(Wq &c[ r<#727/&> K&S @
. q[]r*!2@L&q[^rO1;/!#$@O&>/'%&
)2. I5 /-7 &' &;hc{v^6hw
,CB9Rh2;<4;732@;4B9=<2V6432[

6Uo4@2A6U4C\
$*!7 /&>&' @2. kqW“~W[6W“~WZr*!&
5k ; 9 &P) qb[6bZr ?(&> ,/l*!K ;
9@ ,q~†bŒ„[r6*!) /"&;) &,@Ok,@C&5
[=‚>@!q[~†b•|Zr*!  ; 9@O2" ?'
q„Œƒdp„r=Z„bp|[O7 /#6/-76#o B#6
@4@LV/!2@L7 /72 7=!&>/!,(&N
; 9 &P) b[6bZ&I C#4) 6*!N ; 9) d[
&56#=! ;@ 4&*! @.  7 /q~Œpdpir
W'XYZ[

\,X T)2-. #727/*?7 /2" ?'v[cw
&,*! y2/&> : &I %M&>"$
&, (; 6/> *!&s :(Q C 17 /#R2-.
#727/i>7 /#&>  K&S1 @6/*#=7 /
C@/)&56#=2@L&1 @. q#=a•ip|[r
/-76/-7 6M6*!7 /72 7&>/!/'-=ec

d/-7&>
    k  ;  9  /g  qŒdƒJŒ„r    &56  #=  O  #727/  q#=
ed„<•r&> 2'0 @. q @<•dpiry2/V
&> : 2 %M&s :(Q C 1"/)#727/~s#R
!@$12@L&(&>&9 :*!&9/>6$;
G&/!@/7
J0  .k)2. @O&' &> &() &,@O/!
acc

d6@2. @Oa\c6 0@O/!ac@G ?&() 
! T)2. 2@L7 /72 7/!h\[{7? : T@E-K'
&,#B "N T)7 /2" ?' "5 I' &,*? 0

/!`ccc0zF6F2. 1!5 I&' &;`ccc .#727/zFv^6
[cw

W'XYZZ

`i]K]B22B2R9[O_P
B"RXNM2A624C\

W'XYZa
Metanol , xúc tác H
2
SO
4
Dầu có chỉ
số FFA < 2%
Este hóa
bằng
acid
Dầu hạt cao su
Tách pha
BD
Este hóa
bằng base
Tách pha
Metyl este
Trung hòa
base dư
Làm khan
( khuấy)
Metanol, xúc tác NaOH

T = 45
0
C, τ = 30
T = 50
0
C, τ = 30
Nước nóng, T= 70
0
C
Pha
nhiều
Glyxerin
Pha
nhiều
Glyxerin
Rửa
(khuấy,tách)

I"RXFc5
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&,1&>&(Ik :)&)6(O/% T[[N
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