615 Whitestown Road · P.O. Box 149 · Butler, PA (USA) 16003-0149
Phone: 724/482-2163 · Fax: 724/482-2767 ·· Web Site:
PPT3000 – M-RULE Profile Generation – data form
The PPT3000 – M-Rule shelf-life testing routines are designed to provide material utilization and
predicted shelf-life performance data on bottles at the point of production. The PPT3000 M-Rule shelf-life
prediction software utilizes pressure and expansion data captured by the PPT3000 in conjunction with the
unique attributes of a given bottle. This data is then analyzed by an embedded version of the M-Rule®
Container Performance Model to provide predicted shelf life and material utilization of bottles tested.
Since shelf-life qualities are dependent on a number of critical bottle-specific parameters, it is extremely
important that accurate data be provided to create each unique bottle shelf-life profile for the PPT3000.
One profile is required for each unique bottle design to be tested.
In order to assist you in providing the proper data, we have prepared the following form. This form must
be completed and submitted for each unique bottle tested on the PPT3000. In addition to the data
requested below, please also supply a design drawing of the bottle if available. Data submitted on this
form will be used to create a unique shelf-life profile for the specified bottle. All information supplied
will be treated with strict confidentiality.
Submission Information (Customer to complete)
Agr Contact
Date
Job/Container Information for:
_________________________________________________
(Container Name / Description)
Customer Information
Company Name
Customer Contact
Addr1
Addr2
City
State/Province
Country
Phone:
E-mail
Customer Code
Profile Name
Postal Code
AGR-use only
Order Number
PPT3000 Serial Number
PO Number
Thickness
Shelf Life
SET 1
SET 2
Executable Results Attached
Name
Material Utilization
Report Attached
Date
Rev. 7, 5/30/08
Page 2 of 5
NOTE: The Material (Resin), Finish Design, Base Design, and Closure selections are updated constantly.
If the Resin, Finish Design, Base Design, and/or Closure for the bottle does not appear, specify the Resin,
Finish Design, Base Design, and/or Closure on the questionnaire under “Other”.
Material (Resin)
Polyester: 1,5-PEN
Polyester: 2,6-PEN
Polyester: 2,6-PTN
Blend: MonOxbar
Single Sack™ V700X
6.7% LDR
Polyester: 2,7-PEN
Polyester: Eastman
9921/22
Polyester: Eastman
9921/22W
Polyester: Heat Set PET
– 30% Crystalline
Polyester: Heat Set
PET – 38% Crystalline
Polyester: Invista
1101/1102 series
Polyester: Eastman
CB11/12
Polyester: M&G 8000
series
Polyester: PCT
Polyester:
Poly(glycolic acid)
Polyester: P(DEG)T
Polyester: P(ethylene
phthalate)
Polyester: PBT
Polyester: PET 21%
crystalline
Polyester:
Poly(ethylene isophthalate)
Polyester:
Poly(ethylene
terephthalate)
Polyester: Poly(lactic
acid)
Polyolefin: EVOH 32
mol% ethylene – 27% cryst
Polyolefin: EVOH 32
mol% ethylene – 61% cryst
Polyolefin: LLDPE –
0.92
Polyolefin: O2
Scavenger Concentrate
[193 cc O2/g]
Polyolefin: EVOH 44
mole% ethylene – 27%
cryst
Polyolefin: HDPE – 0.96
Polyolefin: PMMA
Polyolefin: Poly(vinyl
alcohol)
Polyolefin: Poly(vinyl
chloride)
Polyolefin: PP – 0.901
Polyamide: Grivory
FE7103
21
Polyamide: Nylon 6
Polyamide: Nylon MXD-
Polyolefin: Polystyrene
Polyamide: Grivory G
Polyamide: Nylon 6,6
Others: Polyacetal
Others: Polycarbonate
6
Modified Resin:
Constar MonOxbar™ V10
Modified Resin: Constar
MonOxbar™ V6
Modified Resin:
Constar Oxbar™ Multilayer
Scavenger
Other:
Barrier Materials -
Fill in only if barrier
materials are employed on this bottle
Important Note: The PPT-M-Rule shelf-life model
assumes that coatings, and or barrier materials are
applied properly and in place at the specified barrier
levels. Test results will reflect maximum shelf life based on
barrier levels provided in this document.
No barrier materials employed
Coating- internal or external
Coating Type
___________
Barrier Improvement
Factor for O2 (BIF)
_______________
Internal
External
Multiple layer barrier
For Multi-layer Bottles only
Input thickness values below:
Layer
Resin
Page 3 of 5
Weight %
1
Provide thickness data for each layer with
1 being the innermost layer and 5 being
the outermost layer
2
3
4
5
General Data
Item
Value
Unit
Nominal volume
ml.
Brimful capacity
ml.
Surface area
Sq. cm.
Empty package weight
grams
Nominal Thickness (Monolayer)**
mm
Test Temperature
C or F
Expected Shelf Life
** NOTE: it is important to have as
accurate a value as possible for this
parameter. Refer to diagram for
recommended measurement location.
Measure thickness on straight sidewall area with no decorations – take multiple
measurements (8-10) using a high accuracy measurement device such as the
Agr MBT and average the measurement results.
Finish Design
Standard Crimp
28 mm 1716
28 mm PCO
38 mm PCO
38 mm Heat Set
43 mm VHS
28 mm 1716 RefPET
33 mm Sun Coast
48 mm VHJ
38 mm Cold Fill
28 mm SP400
PTI crimp
18 mm
43 mm VHS Lt. Wt.
Petaloid
Champagne
Heatset Champagne
Push-Up
Crimp top
28 mm Alcoa
28 mm White Cap
28 mm Zapata
28/400 Zeller
28-4CO Top Seal
33 mm O-I
33 mm Sun Coast
38 mm Alcoa
38 mm White Cap
43 mm Alcoa
Other:
Base Design
Heatset Petaloid
Flat-bottom
Other:
Closure
Page 4 of 5
43 mm White Cap
Other:
Closure Material
Polypropylene
High Density
Polyethylene
Metal (impermeable)
Other:
Co2 Test
Protocol
Coke Standard Test
Pepsi Standard Test
4.0-3.3 gas volume @ 22º C
FTIR – empty bottle
4.0-3.3 gas volume @ 22º C
Zahm-Nagle method --- filled
Custom test protocol
Provide details below
Required data for Custom test protocol if not using Coke or Pepsi standard tests
Initial carbonation level: ________________________________ volumes
Upper Carbonation Spec:
_____________________________ volumes
Lower Carbonation Spec:
_____________________________ volumes
Reference Test Method _______________________________ (FTIR, Zahm-Nagle, etc.)
Test Temperature _________________
Package Fill Volume:
Nominal
Empty
Brimful (defines how test is to be run)
O2 Test
Protocol
Initial level: _____________________ value _____________________ units
End level:
_____________________ value _____________________ units
Test Temperature _________________
Empty or Filled Container? ______________________
Shelf-life values to be based on the following method:
If both are chosen, 2 profiles will
be provided. Tests are performed
individually, not combined.
CO2 out gassing (egress)
O2 ingress
Please return completed form to the following:
Page 5 of 5